special session on mgb2
 
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Post deadline Session on MgB2

Talks 60 - 79

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Table of Contents
  Talks:   1-19     20-39     40-59      60-79
Talk 60 Magnetic Transitions in MgB2
Talk 61 High Temporal Stability of Supercurrents in MgB2
Talk 62 Current transport and magnetic relaxation near and below the irreversibility
Talk 63 Critical Currents and Flux Creep in MgB2
Talk 64 Magneto-optical study of flux penetration in MgB2
Talk 65 Temperature dependence of the intergranular critical currents in MnB2 ceramic
Talk 66 Giant quantum fluctuation of vortices in the new superconductor MgB2
Talk 67 The new superconductors.
Talk 68 The upper critical field problem in MgB2
Talk 69 Ab-initio calculations of lattice dynamics and electron-phonon coupling in MgB2
Talk 70 Measurement of the B
Talk 71 dHvA measurements in MgB2
Talk 72 Soft X-ray Spectroscopy measurements of MgB2 at the B-K edge
Talk 73 Investigation of Electronic Excitations in MgB2 by Raman Spectroscopy
Talk 74 High-Frequency Studies of MgB2
Talk 75 Pressure Effects of MgB2 Superconductors on Its Tc and Crystal Lattice
Talk 76 Carbon substitution effect in MgB2
Talk 77 Improved superconducting thin films of MgB2 on Si
Talk 78 Superconducting MgB2 thin films by pulsed laser deposition.
Talk 79 Te Amplification by Shape Resonance

 

Talk 60

Magnetic Transitions in MgB2 

L.D. Cooley, S. Patnaik, D.C. Larbalestier, A. Gurevich, X.Y. Cai, A.A. Polyanskii, M. Rikel, J.Y. Jiang, X. Song, S. E. Babcock, C.B. Eom, and E.E. Hellstrom, Applied Superconductivity Center, University of Wisconsin–Madison. 

Magnetization data from 0-14 T and 4.2-45 K were acquired for several MgB2 samples obtained from different sources.  The derived values of the upper critical field Hc2 and the field HK at which Kramer plots extrapolate to zero flux pinning show little variation, despite the range of sample homogeneity and the differences in preparation.  Since some samples were reacted with an excess of Mg while others were made in an excess of B, these data suggest there is very little variation of the stoichiometry of the primary superconducting regions.  The variation of HK(T) is linear and proportional to Hc2(T), which is not the expected behavior for an irreversibility line.  A tail is also visible on all Kramer plots above HK, indicating that residual irreversible current loops persist to near Hc2.

 


Talk 61

High Temporal Stability of Supercurrents in MgB2

J.R. THOMPSON, ORNL/University of Tennessee, M. PARANTHAMAN, D.K. CHRISTEN, Oak Ridge National Lab, K.D. SORGE, H.J. KIM, University of Tennessee, J.G. OSSANDON, University of Talca, Chile

Fine grained polycrystalline samples of MgB2 superconductor were synthesized by reaction of the pure elements at 890 ˚C for 2 h in a sealed Ta tube within an evacuated quartz ampule. Sintered or powdered materials, containing <5 % of impurity phases per X-ray powder diffractometry, had a sharp transition with a midpoint Tc = 38.5 K. The supercurrent density J(T,H,t) in the vortex state was studied as function of temperature T, magnetic field H, and time t. The current J is highly stable  in time,e.g., the “flux creep” rate S = -dln(J)/dln(t) ≤ 0.02 in fields of 1 Tesla, for temperatures up to Tc/2. Compared with high-Tc’s, the decay rate S is smaller by a factor of 3-10 or more. In addition, the persistent current density J decreases approximately linearly with T, in contrast to the quasi-exponential falloff in HTSC’s; this is another manifestation of the highly stable J(t).

 


Talk 62

Current transport and magnetic relaxation near and below the irreversibility line of MgB2

X.Y. Cai, A. Gurevich, S. Patnaik, A.A. Polyanskii, M. Rikel, J.Y. Jiang, L.D. Cooley, C.B. Eom, E.E. Hellstrom, and D.C. Larbalestier, Applied Superconductivity Center, University of Wisconsin–Madison, S.L. Bud’ko, C. Petrovic, G. Lapertot, C.E. Cunningham, and P.C. Canfield, Ames National Laboratory. 

We performed magnetic flux creep and transport measurements on sintered MgB2 samples in magnetic fields near and below the irreversibility line B* » 0.2(Tc – T) [Tesla]. The dimensionless flux creep rate s(T,B) = dlnM/dlnt was found to decrease with the magnetic field B and temperature T, from s ~ 10-2 at B << B* to s ~ 1 at B » B*. Resistive measurements near B* enabled us to trace the crossover from a nonlinear current-voltage characteristic below B* to the flux flow behavior above B*.

 


Talk 63

Critical Currents and Flux Creep in MgB2 (no slides, audio only)

Garry Perkins, Yura Bugoslavsky, Max Polichetti, Xiaoding Qi, Alexei Zhukov, Lesley Cohen, Judith Driscoll. Centre for High Temperature Superconductivity, Imperial College, London SW7 2BZ, UK

We report detailed measurements on small (~ 100 micron) polycrystalline fragments of MgB2 of critical current densities Jc and flux creep rate S.  The natural grain boundaries within the fragments appear fully transparent to supercurrent. Within the framework of collective pinning theory that has been applied to HTS materials, the dependences of Jc and S on field suggest a catastrophic decline in pinning energy of pure MgB2 with increasing field.

 


Talk 64

Magneto-optical study of flux penetration in MgB2

A.A. Polyanskii, J.Y. Jiang, M. Rikel, S. Patnaik, X.Y. Cai, L.D. Cooley, A. Gurevich, C.B. Eom, E.E. Hellstrom, and D.C. Larbalestier, Applied Superconductivity Center, University of Wisconsin–Madison, S.L. Bud’ko, C. Petrovic, G. Lapertot, C.E. Cunningham, and P.C. Canfield, Ames National Laboratory. 

Magneto-optical (MO) studies of flux penetration in sintered MgB2 samples and MgB2 wires were performed. The sintered samples showed well developed roof patterns, rather uniform critical state and Bean-like flux profiles, which enabled us to extract bulk magnetization current density Jc(T) in the temperature range 12K < T < Tc and magnetic fields, H < 1200 Oe.  The wires showed much more nonuniform flux penetration due to material inhomogeneities and microcracks. From the MO flux profiles we obtained the local Jc values of order 105 A/cm2, in agreement with magnetization measurements.

 


Talk 65

Temperature dependence of the intergranular critical currents in MnB2 ceramic samples.

V.K.Vlasko-Vlasov, U.Welp, G.W.Crabtree, D.J.Miller, D.Hinks  Argonne National Laboratory, Argonne, IL

Magneto-optical measurements of the flux distributions in MnB2 samples reveal regions of high critical currents connected by noticeably weaker current links. This is in accordance with polarized optics and electron microscopy pictures showing dense and less dense compacts of small single crystal MnB2 grains. From the average slopes of the trapped flux profiles the weak intergranular currents, limiting the current carrying ability of the samples, and their temperature dependence were determined. Currents in the well coupled regions are estimated to be an order of magnitude larger.  

 


Talk 66

Giant quantum fluctuation of vortices in the new superconductor MgB2

H. H. Wen*, S. L. Li, Z. W. Zhao, Y. M. Ni, Z. A. Ren, G. C. Che, H. P. Yang, Z. Y. Liu and Z. X. Zhao. National Lab for Superconductivity, Institute of Physics and Chinese Academy of Sciences, P. O. Box 603, Beijing 100080, P. R. China

The recently discovered new superconductor MgB2 generates enormous interests in the field of superconductivity. One big issue concerns in which region on the field-temperature phase diagram it can carry large critical current density ( jc ) and thus can be used in the future for industry. This jc is controlled by the mobility of the magnetic vortex tubes ( vortices ) and vanishes at the melting line between the vortex solid and liquid. This melting can be induced by strong fluctuation of the vortex position by either thermal or quantum effect. At T = 0 K only the quantum fluctuation is left. In this report we present the evidence for a vortex quantum liquid induced by giant quantum fluctuation effect at zero K. Further investigation on the magnetic relaxation at different fields may indicate that the melting at a finite temperature is also governed by this effect posing a strong limit to the application of this new superconductor in a high field.

 


Talk 67

The new superconductors. (no slides, audio only) 

John D. Dow, Arizona State University

Two new potential superconductors have raised considerable interest recently: MgB(2) (T(C)=39 K) [1] and Ag(x)Pb(6)CO(9) (T(C)=342 K) [2].  Both materials appear to have hole carriers.  MgB(2) appears to be a “low-temperature” phonon superconductor (with a rather high temperature), and Ag(x)Pb(6)CO(9) may be a genuine “high-temperature” superconductor, if its superconductivity is confirmed.

[1] J. Nagamatsu, N. Nakagawa, T. Muranaka, Y. Zenitani, and J. Akimitsu,

“Superconductivity at 39 K in magnesium diboride,” to be published.

[2] D. Djurek, Z. Meduniae, A. Tonejc, and M. Paljeviae, “Onset of superconductivity at 342 K in a novel chain conductor Ag(x)Pb(6)CO(9) (0.7<x<1),” to be published.

 


Talk 68

The upper critical field problem in MgB2

H. ROSNER, W.E. PICKETT, Department of Physics, UC Davis, S. SHULGA, S. -L. DRECHSLER, H. ESCHRIG, Institute for Solid State and Material Research Dresden, Germany.

The upper critical field HC2(T) for MgB2 is analyzed in terms of single and multi-band Eliashberg models. The relatively high value of HC2(0) ≈ 14 to 18 T can be understood, if a strongly coupled subgroup of heavy quasiparticles is involved in the superconductivity. The sizable coupling to both low- and high-frequency bosons is essential. This picture is supported by LDA calculations of Fermi velocity distribution over different sheets of the Fermi surface with special emphasis on the hole tubes. The possible origin of anharmonic soft modes is briefly discussed. Similarities and differences with transition metal borocarbides are figured out.

 


Talk 69

Ab-initio calculations of lattice dynamics and electron-phonon coupling in MgB2

V. OZOLINS and M. VAN SCHILFGAARDE, Sandia National Laboratories, Livermore, California. 

We have carried out first-principles linear response calculations of phonon densities of states and electron-phonon interaction in MgB2. Complete phonon densities of states, electron-phonon spectral function a2F(w) and l for MgB2 will be presented. The nature of the lattice dynamics and its relation to the strong electron-phonon coupling in this system will be discussed.

 


Talk 70

Measurement of the B 2p Valence Band Electronic Structure of MgB2 using High Resolution Soft X-ray Emission Spectroscopy

CORMAC McGUINNESS and KEVIN E. SMITH, Department of Physics, Boston University, 590 Commonwealth Ave, Boston, MA 02215, J. GUO and J. NORDGREN, Department of Physics, Uppsala University, Box 530, 75121 Uppsala, Sweden, T. VOGT, J. REILLY, J. F. TU, G. SCHNEIDER and P. D. JOHNSON, Department of Physics, Brookhaven National Laboratory, Upton, NY 11973.

The valence band electronic structure of MgB2 has been measured using soft x-ray emission (SXE) and soft x-ray absorption (SXA) spectroscopies.  SXE provides direct measurement of the occupied, elementally resolved, partial density of states (PDOS) in solids.  SXE is bulk sensitive due to a sampling depth of approximately 1000 Å, and is insensitive to the degree of sample crystallinity.  The room temperature B 2p valence band PDOS was obtained by recording the radiative de-excitation of a B 1s core hole.  The B 1s hole was created with monochromatic soft x-ray radiation from an undulator device at the Advanced Light Source.  Photon energies well above the excitation threshold were used in the PDOS measurement.  The SXE measurements of the occupied PDOS agree well with a tight binding calculation. Likewise, the unoccupied B 2p PDOS measured using SXA is similar to the calculated PDOS with one exception: an intense narrow absorption feature is observed just above the absorption threshold.  We speculate that this feature is excitonic in nature. Resonant excitation at this absorption energy results in strong inelastic scattering and a dramatic change in the observed x-ray emission spectrum.

 


Talk 71

dHvA measurements in MgB2

E. C. Palm, S. W. Tozer, Donavan Hall, and T. P. Murphy, National High Magnetic Field Laboratory Florida State University, Tallahassee, FL, S. L. Bud’ko, G. Lapertot, C. Petrovic, C. E. Cunningham, and P. C. Canfield, Ames Laboratory and Dept. of Physics and Astronomy, Iowa State University

We report de Haas - van Alphen (dHvA) measurements made on isotopically pure Mg11B2 powder and dense MgB2 wires. The powder samples were mixed with epoxy and oriented in a 33 T field while the epoxy cured. The measurements were performed at temperatures between 0.5 K and 40 K in magnetic fields up to 33 T using a high quality torque cantilever magnetometer. Typical data, measured frequencies of the oscillations and effective masses of principle orbits, will be presented.

 


Talk 72

Soft X-ray Spectroscopy measurements of MgB2 at the B-K edge

T.A. CALLCOTT, L. LIN, G.T. WOODS, J. R. THOMPSON, Univ. of Tennessee, and M. PARANTHAMAN, Oak Ridge National Laboratory

We report soft x-ray absorption and fluorescence measurements at the boron K-edge of superconducting MgB2.  Three notable features are found.  The measurements confirm a high density of B p-states at the Fermi edge and extending to approximately 0.8 eV above the edge, which is derived from B-s (2pxy). orbitals They also show a strong exciton feature indicating strong localization in the out-of-plane p (2pz).  orbiatls.  Finally, a second excitonic feature is observed that derives from boron oxide contamination of the sample.

 


Talk 73

Investigation of Electronic Excitations in MgB2 by Raman Spectroscopy

X. K. CHEN, M. J. KONSTANTINOVIC, J. C. IRWIN, Department of Physics, Simon Fraser University, Burnaby, B.C., V5A 1S6, Canada; J. P. FRANCK, Department of Physics, University of Alberta, Edmonton, A.B., T6G 2J1, Canada.

The Raman spectra of polycrystalline MgB2 have been measured from 50 cm-1 to 1200 cm-1 at temperatures above and below Tc, using parallel and crossed polarization scattering geometries.  A broad continuum due to scattering from electronic excitations was found to behave similarly to the electronic continua observed in the high-Tc cuprates.  When the temperature was decreased below Tc, a superconductivity-induced redistribution in the continuum was observed.  A pair-breaking peak at 110 cm-1 due to excitations across the superconducting gap appeared in both scattering geometries.  The peak frequency and its polarization dependence indicate an isotropic s-wave gap with 2D/kBT»4.2, which corresponds to the strong-coupling regime.

 


Talk 74

High-Frequency Studies of MgB2

S. E. Lofland, Dept. of Physics and Chemistry, Rowan University, Glassboro, NJ, Dept. of Physics, University of Maryland, College Park, S. D. Tyagi, Dept. of Physics, Drexel University, Philadelphia, PA, K. V. Ramanajuchary, M. Botsford, Dept. of Physics and Chemistry, Rowan University, Glassboro, NJ

We present microwave absorption and susceptibility studies of MgB2.  We find that the absorption is well described by the London model, yielding a reasonable for the penetration depth.  In addition, we find that the number of weak links is much smaller than in HTSC; however, they are not completely negligible.  Frequency-dependent susceptibility studies show that the vortex pinning is very strong.

 


Talk 75

Pressure Effects of MgB2 Superconductors on Its Tc and Crystal Lattice

J. Tang,1 A. Matsushita,1 Y. Takano,1 K. Togano,1 H. Kito,2 H. Ihara,2 L.-C. Qin 3

"Times New Roman"'>1 National Research Institute for Metals, 1-2-1 Sengen, Tsukuba 305-0047, Japan

2 Electrotechnical Laboratory, 1-1-4 Umezono, Tsukuba 305-8568, Japan

3 JST-ICORP Nanotubulite Project, c/o NEC Corp., Tsukuba 305-8501, Japan

Hydrostatic pressure up to 10 GPa has been applied to determine the dependence of transition temperature Tc and lattice properties of an MgB2 superconducting material that is prepared by high pressure (3.5 GPa) and high temperature (1000 ºC). This material shows narrowed region in temperature during the transition from normal state to superconducting state. The transition temperature Tc decreases with increasing pressure linearly at a rate of 1.03 K/GPa. The crystal lattice properties, measured with a diamond anvil cell using in situ synchrotron X-ray diffraction, show anisotropy with its c-axis being more compressible than the a-axis.

Correspondence: tang@nrim.go.jp

 


Talk 76

Carbon substitution effect in MgB2

Jai Seok Ahn1 and Eun Jip Choi1,2,

1 Center for Strongly Correlated Materials Research, Seoul National University, Seoul 151-742, Korea,

2 Department of Physics, University of Seoul, Seoul 130-743, Korea

We investigated carbon substitution effect on boron plane of superconducting MgB2. MgB2 and MgB1.8C0.2 samples are synthesized under high pressure furnace. MgB1.8C0.2 are characterized as AlB2-type single phase with smaller B-B distance. During the superconducting transition, two distinct onset temperatures are observed in MgB1.8C0.2.

 


Talk 77

Improved superconducting thin films of MgB2 on Si.

A. BRINKMAN, D. MIJATOVIC, G. RIJNDERS, V. LECA, H.J.H. SMILDE, I. OOMEN, A. A. GOLUBOV, F. ROESTHUIS, S. HARKEMA, H. HILGENKAMP, D.H.A. BLANK and H. ROGALLA. Low Temperature Division, MESA+ Research Institute and Faculty of Applied Physics, University of Twente, Enschede, The Netherlands, and C.A.J. DAMEN, TSST, Hengelo, The Netherlands.

In a follow-up of our cond-mat/0103198, new results will be presented on improved superconducting thin films prepared on Si-substrates, using pulsed laser deposition from a target composed of a mixture of Mg and MgB2 powders. The films are deposited at room temperature and subsequently in-situ post-annealed. More information will be presented on the optimization of the background pressure of Ar gas in the deposition-chamber, for which the color of the plasma is used as indicator. 

 


Talk 78

Superconducting MgB2 thin films by pulsed laser deposition.

S. R. SHINDE, S. B. OGALE, R. P. SHARMA, R. L. GREENE and T. VENKATESAN, Center for Superconductivity Research, Department of Physics, University of Maryland, College Park, MD 20742-4111, P. C. CANFIELD, S. L. BUD’KO, G. LAPERTOT, Ames Laboratory, U. S. Department of Energy and Department of Physics and Astronomy, Iowa State University, Ames, Iowa 50011

Thin films of MgB2 exhibiting susceptibility and resistivity transitions (TC) between 20-30 K are grown by in situ pulsed laser deposition process. Different approaches involving ablation from a stoichiometric target under different growth conditions, as well as multiplayer deposition involving interposed Mg layers are examined and analyzed. Other strategies such as post-deposition-annealing at 900 C with excess Mg (an ex situ process) are also studied. Magnetic measurements on such samples show TC as high as 38 K. These data will be presented and discussed. 

 


Talk 79

Te Amplification by Shape Resonance

A. Bianconi*, D. Di Castro, S. Agrestini, G. Campi, N. L. Saini, Department of Physics, and IBFM University of Roma "La Sapienza", P. le Aldo Moro 2, 00185 Roma, Italy. A. Saccone, S. De Negri, M. Giovannini, Dipartimento di Chimica e Chimica Industriale, Universite di Genova, Via Dodecaneso 31, 16146 Genova, Italy. We have studied the variation of Tc as a function of charge density and lattice parameters in Al doped MgB2 superconducting samples. We show that high Tc superconductivity in MgB2 is realized by tuning the chemical potential near a "shape resonance" as described in the patent for "high-temperature superconductors made by metal heterostructures at the atomic limit". The metallic MgB2 heterostucture at the atomic limit made by chemical reactions is used for Tc amplification according with the claim of the patent at the n=2 "shape resonance" for the superlattice of boron monolayers. For further information: Presenting author, email: http://www.superstripes.com antonio.bianconi@roma1.infn.it